The strong base created an anion from an ester of Miltonic acid. The ion reacted with browbeaten which was also in the action solution to give the product.
The yield product was a butyl derivative of Miltonic ester that was isolated by adding water to the reaction solution, and extracting with ether. The ether was dried and evaporated to give the product. Procedures: 0. Egg of tricaprylmethylammonlum chloride, 0. Egg of 1- browbeaten, 0. Egg fatherly maltose, and 0. Egg of potassium carbonate were mixed in a ml long-necked, round-bottom flask. The apparatus was set up according to figure 42. 1 . The distillation column was attached to be used as an alarm condenser in order for the reaction solution to reflux.
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The flask contacting the reaction solution was heated. The solution was cool to room temperature for a few minutes, and put Into Ice. The solution was transferred to a drawn off. The aqueous layer was extracted with two portions of 1. ml of ether. The combined organic extracts were dried over anhydrous calcium chloride pellets. The ether was removed from the drying agent, and ether was finished drying over calcium sulfate. The dry ether solutions were placed in a “dry’, tarred ml long- kicked, round-bottom flask.
The ether was removed by distillation or evaporation in the hood. The last remaining of ether was removed by connecting the flask to an aspirator. The product was weighted. The theoretical and percentage yield was calculated. A TTL plate in 30% hexane and 40% DC was conducted to compare the product with pure ethyl n-battlemented and starting materials ethyl Malone and browbeaten. Data: Reaction: Ethyl n-Battlemented Compound Transmogrification’s chloride (ammonium salt) Ethyl Malone I-broom- butane